Name | carbamoyl chloride Carbamyl chloride |
Synonyms | MCC Urea chloride chloroformamide carbamic chloride Carbamyl chloride carbamyl chloride carbamoyl chloride Carbaminoyl chloride N-Methylchloroformamide Carbamic chloride (9CI) N-chloro-N-methylformamide N-Methylaminoformyl chloride |
CAS | 463-72-9 |
EINECS | 207-342-1 |
InChI | InChI=1/CH2ClNO/c2-1(3)4/h(H2,3,4) |
Molecular Formula | CH2ClNO |
Molar Mass | 79.49 |
Density | 1.3273 (rough estimate) |
Melting Point | 90℃ |
Boling Point | bp 61-62° (decompn) |
Flash Point | 35.6°C |
Vapor Presure | 7.77mmHg at 25°C |
pKa | 11.60±0.50(Predicted) |
Refractive Index | 1.4480 (estimate) |
Physical and Chemical Properties | Character crystals. melting point 90 ℃ |
Use | For carbamate pesticide intermediates |
Raw Materials | Chlorine Methylamine |
This product is a crystal with a melting point of about 90 °c.
results from the interaction of methylamine with phosgene. The 40% methylamine aqueous solution was vaporized, dried and mixed with phosgene at a ratio of 1:1.3, methylamine at 4 m3 /h and phosgene at a ratio of 8. The speed of 6 r13/h (content of 60% ~ 70%) respectively into the preheater preheating, methyl amine preheating temperature control in 220~260 ℃, phosgene control in 200~240 ℃, the two preheated gases enter the Venturi and are synthesized at 280-300 °c to give methyl carbamoyl chloride. Then, carbon tetrachloride (or chlorobenzene solution) is recycled and absorbed at 0-20 ° C. To obtain about 10% of the carbamoyl chloride in carbon tetrachloride (or chlorobenzene) solution, which is distilled to obtain the finished product.
pesticides carbamate insecticides and herbicides intermediates.
This product is packed in polypropylene or polyethylene large diameter plastic barrel with a net weight of 50kg per barrel.
Use | Used as an intermediate for carbamate pesticides |
Production method | is obtained by the interaction of methylamine and phosgene. The 40% methylamine aqueous solution is vaporized, and after drying, it is mixed with phosgene at a ratio (volume) of 1:1:3, methylamine at 4 m3/h, and phosgene at a speed of 8.6 m3/h (content 60% ~ 70%). The preheating temperature of methylamine is controlled at 220~260 ℃, and the phosgene is controlled at 200~240 ℃. The two preheated gases enter the venturi tube, the gas methylcarbamoyl chloride was synthesized at 280~300 ℃. Then carbon tetrachloride (or chlorobenzene solution) is used for cyclic absorption at 0~20 ℃ to obtain about 10% carbon tetrachloride (or chlorobenzene) solution of methylcarbamoyl chloride, which is distilled and rectified to obtain the finished product. |